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S after rehydration (usually 10?0 ). Samples were digested overnight at 37 . MALDI-TOF analysis A 1.2 aliquot of the digestion solution was pipetted onto an AnchorChipTM 384/600 target (Bruker Daltonics GmbH, Bremen, Germany) as described [18]: 0.6 of matrix solution (2 mg -Cyano-4-hydroxycinnamic acid [CHCA, Bruker Daltonik GmbH] dissolved in 0.33 ml of 2.5 aqueous TFA and 0.66 ml acetonitr

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